Qualitative inorganic analysis, inorganic preparations and elementarycrystal chemistry

Course Code: 2860, Course Title: Qualitative inorganic analysis, inorganic preparations and elementarycrystal chemistry Marks 100, 4 Credits, 60 Lectures 1.Safety: The twelve rules of safety, safety in the laboratory. 2.Purification and Preparation of Inorganic Compounds: (i)Purification of commercial NaCl by recrystallization and salting out processes, (ii)Preparation of ferrous sulphate FeSO4.7H2O, Mohr’s salt [FeSO4. (NH4)2SO4. 6H2O], potash alum [K2SO4. Al2(SO4)3. 24H2O], chrome alum [K2SO4. Cr2(SO4)3. 24H2O], sodium carbonate Na2CO3. (iii)A cycle of reactions from Cu0 through Cu0 via copper nitrate, hydroxide, oxide, and sulphate as intermediates in succession. 3.Model Making: Seven crystal systems model. 4.Systematic Semimicro Qualitative Analysis of Inorganic Salts: Identification of inorganic basic and acid radicals, 5 radicals in a mixture taking at least two from both ion types. Books Recommended: 1.A Text-Book of Macro and Semimicro Qualitative Inorganic Analysis, A. I. Vogel, 4th edition, Longmans, Green and Co. Ltd. 2.Semimicro Qualitative Analysis, F. J. Welcher and R. B. Hahn, D. Van Nostrand Co. Inc. 3.Qualitative Analysis, V. Alexeyev, Mir Publishers.